4.5 Article

Fast microtomography using high energy synchrotron radiation -: art. no. 043702

Journal

REVIEW OF SCIENTIFIC INSTRUMENTS
Volume 76, Issue 4, Pages -

Publisher

AMER INST PHYSICS
DOI: 10.1063/1.1884194

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At the High Energy Beamline ID15A at the European Synchrotron Radiation Facility we have developed a fast three-dimensional x-ray microtomography system, which acquires a complete dataset in typically less than 10 s. This unprecedented speed is achieved by combining a high efficiency phosphor screen, a reflecting microscope objective and a fast charge coupled device detector with the very intense high-energy white beam radiation provided by a wiggler source. The achieved spatial resolution is 2 mu m. The available x-ray energy spectrum spans from 20 to 250 keV and can therefore be used for low and high Z materials. The spectrum can be modified by inserting different filters into the x-ray beam in order to optimize the signal-to-noise ratio and to avoid beam-hardening artifacts. Different phosphors with different energy sensitivity can be used. The very high speed allows in situ studies of systems evolving on the time scale of a few seconds or minutes. Three examples are given on sintering of metallic powders, solidification of binary alloys and liquid front propagation in granular materials. (C) American Institute of Physics.

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