Journal
NANO LETTERS
Volume 5, Issue 4, Pages 685-691Publisher
AMER CHEMICAL SOC
DOI: 10.1021/nl050097t
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A continuous flow microreactor was used for the synthesis of gold nanoparticles (5 to 50 nm) directly from a gold salt (HAuCl4) and a reducing agent (ascorbic acid). Experimental parameters were optimized to obtain narrow size distributions, which were at average two times narrower than those obtained in a conventional synthesis. Additionally, two approaches, i.e., elevation of pH during reaction and hydrophobization of internal reactor surfaces were tested to suppress reactor fouling.
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