Journal
CHEMISTRY OF MATERIALS
Volume 17, Issue 7, Pages 1797-1802Publisher
AMER CHEMICAL SOC
DOI: 10.1021/cm048032z
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We report on a very simple, efficient, and economical synthetic technique that produces SiC of a high surface area, and under different conditions of a silicon carbide-carbon nanocomposite (SCCN) at a relatively low temperature. A high yield of pure products is obtained in a one-stage, single-precursor reaction, without a catalyst. The cracking/dissociation of a triethylsilane precursor is carried out separately in a closed vessel cell (Swagelok) that was heated at 800 degrees C for 3 h, yielding SCCN, and at 1000 degrees C for 3 h, yielding SiC. This synthetic process is termed RAPET (Reactions under Autogenic Pressure at Elevated Temperature) process for the synthesis of nanomaterials.
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