Journal
ORGANIC LETTERS
Volume 7, Issue 8, Pages 1593-1596Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol050289v
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- NCI NIH HHS [R01 CA090383] Funding Source: Medline
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Additions of chiral allenylzinc and indium reagents to N-Boc alaninal were examined as a possible route to a C20-C26 segment of superstolide A. Allenylzinc reagents, prepared in situ by palladiozincation of (R)- and (S)-5-pivalyloxy-3-butyn-2-ol mesylate, showed excellent reagent control to afford the anti,syn and anti,anti diastereomers as the nearly exclusive adducts.
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