Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 70, Issue 8, Pages 3339-3341Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo050090w
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A PdCl2-catalyzed cis-chloropalladation-cyclization reaction of various 1,6-enyne substrates was developed. This Pd-catalyzed enyne cyclization reaction represents a new route for the synthesis of stereodefined alpha-halomethylene-gamma-butyrolactones, lactams, tetrahydrofurans, and cyclopentanes. A mechanism involving a neighboring coordination group is proposed to explain the experiment results.
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