Journal
APPLIED MAGNETIC RESONANCE
Volume 45, Issue 1, Pages 9-17Publisher
SPRINGER WIEN
DOI: 10.1007/s00723-013-0502-6
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Funding
- Basic Science Research program through the National Research Foundation of Korea (NRF)
- Ministry of Education, Science, and Technology [2012001763]
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To clarify the nature of microscopic structural changes of N(CH3)(4)CdCl3 at high temperatures, the nuclear magnetic resonance (NMR) spectra of the protons and carbons in N(CH3)(4)CdCl3 were measured. NMR studies of the H-1 and C-13 spin-lattice relaxation time, T (1 rho), in the rotating frame were also performed. No changes in the T (1 rho) of H-1 and C-13 associated with the N(CH3)(4) groups were observed at the high-temperature transition from phase I to phase I'. However, the N-14 NMR spectra reflected changes in the structural geometry during the transition to phase I', indicating that this transition is driven by N(CH3)(4).
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