4.5 Article

One-pot acetalation-acetylation of sugar derivatives employing perchloric acid immobilised on silica

Journal

CARBOHYDRATE RESEARCH
Volume 340, Issue 6, Pages 1075-1080

Publisher

ELSEVIER SCI LTD
DOI: 10.1016/j.carres.2005.02.012

Keywords

perchloric acid on silica; acetal-ketal; acetylation

Funding

  1. Biotechnology and Biological Sciences Research Council [BBS/E/J/000C0618] Funding Source: Medline

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Perchloric acid immobilised on silica gel has been used as an efficient promoter for per-O-acetylation, and acetalation and subsequent O-acetylation of glycosides and thioglycosides in one-pot using stoichiometric reagents. (c) 2005 Elsevier Ltd. All rights reserved.

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