Journal
ANALYTICA CHIMICA ACTA
Volume 538, Issue 1-2, Pages 71-76Publisher
ELSEVIER
DOI: 10.1016/j.aca.2005.02.028
Keywords
pressurized liquid extraction; liquid chromatography; tocopherol; tocotrienol; palm oil
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Pressurized liquid extraction (PLE) along with normal phase liquid chromatography (NPLC) is evaluated as a new approach for the determination of P-carotene and Vitamin E isomers in residue oil obtained from palm pressed fiber (PPF). The relative extraction recoveries obtained by optimized PLE were found to be equivalent (similar to 100%) to conventional Soxhlet extraction. Optimized PLE was obtained (5g of sample, 80 degrees C, 1500 psi, 2 x 10 min static extractions with flush volume 50%) combined with NPLC system. Typical extractions give 3.7-4.0 mg ml(-1) of Vitamin E isomers and P-carotene of 3.3-3.5 mg ml(-1), which is similar to or greater than classical Soxhlet extraction with n-hexane or chloroform. The new developed method demonstrated an acceptable performance with good efficiency in terms of total extraction time, total solvent usage, total P-carotene and Vitamin E isomers contents as well as exceptional method repeatability. (c) 2005 Published by Elsevier B.V.
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