Journal
ORGANIC LETTERS
Volume 7, Issue 10, Pages 1999-2002Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol0504796
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Phosphate monoesters are synthesized from a mixture of phosphoric acid (1 or 2 equiv) and alcohols (1 equiv) in the presence of tributylamine. The reaction is promoted by nucleophilic bases such as N-alkylimidazole and 4-(N,N-dialkylamino)pyridine. 2',3'-O-Isopropylidene ribonucleosides are selectively converted to their 5'-monophosphates without the protection of amino groups in nucleobases.
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