Journal
JOURNAL OF COORDINATION CHEMISTRY
Volume 58, Issue 8, Pages 653-659Publisher
TAYLOR & FRANCIS LTD
DOI: 10.1080/00958970412331336295
Keywords
4-aminopyridine; mononuclear Cu(II) complex; crystal structure; IR-LD analysis
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A new mononuclear Cu(II) complex of 4-aminopyridine (4AP), [Cu(4AP)(4)]Cl-2 center dot 2CH(3)OH (1), was obtained and structurally characterized by single-crystal X-ray diffraction methods. The complex is square-planar involving four monodentate 4AP molecules coordinated through the N-py atoms. A solid-state linear-dichroic spectroscopic analysis (IR-LD) as a suspension in a nematic liquid crystal was carried out over the 4000-400 cm(-1) range and determined stereochemical parameters compared crystallographic data. Detailed IR characteristics are reported.
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