Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 70, Issue 11, Pages 4531-4534Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo050191u
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The cyclization of 2-(1-alkynyl)-2-alken-1-ones 1 proceeded very smoothly in the presence of alcohols 2 with a catalytic amount of Cu(I)Br in DMF at 80 degrees C, leading to the formation of highly substituted furans 3. The catalytic system reported herein is easy to handle, compared to the previously known system wherein the reaction between 1 and 2 needed to use moisture sensitive gold(III) chloride.
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