Journal
SYNLETT
Volume -, Issue 9, Pages 1453-1455Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-2005-868492
Keywords
alcohols; esters; hydrogen transfer; iridium catalyst; oxidative dimerization
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Oxidative dimerization of primary alcohols with 2-butanone in the presence of an amino alcohol-based Ir bifunctional catalyst was accomplished for the first time. The reaction proceeds with 1-2 mol% of the catalyst and 0.3 mol equivalents of K2CO3 in 2-butanone at room temperature to give the corresponding dimeric esters in 30-93% yield.
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