Journal
APPLIED CATALYSIS B-ENVIRONMENTAL
Volume 102, Issue 3-4, Pages 417-423Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.apcatb.2010.12.014
Keywords
Carbothermal reduction; ZnO-ZnS/C; Visible light responsive photocatalyst
Funding
- National Natural Science Foundation of China [20901012]
- Science & Technology Foundation of Liaoning of China [1050300]
- Science & Technology Foundation of Education Department of Liaoning Province [05L074, 05L081]
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A new visible light responsive ZnO-ZnS/C photocatalysts have been successfully synthesized by a simple heat-treating procedure using ZnSO4 as single precursor for the first time. The resultant samples were characterized by X-ray diffraction, transmission electron microscopy, X-ray photoelectron spectroscopy and BET surface area measurement. The results showed that the ZnO-ZnS/C catalysts were directly formed by thermal decomposition of ZnSO4 impregnated on the activated carbon at high temperature under open atmospheric conditions. Here, a possible growth mechanism of the coupled ZnO-ZnS/C photocatalysts was proposed. Activated carbon played both reducing agent and support role in formation of ZnO-ZnS/C catalysts. The photocatalytic activities of catalysts were investigated by degrading reactive brilliant blue K-3R under visible light irradiation. The synthesized catalysts showed excellent photocatalytic activity compared with ZnO/C and pure ZnO, which is ascribed to the formation of ZnO-ZnS heterojunctions in catalysts. Furthermore, influences of preparation conditions on photocatalytic activity of the catalysts have been investigated. (C) 2010 Elsevier B.V. All rights reserved.
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