Journal
TETRAHEDRON LETTERS
Volume 46, Issue 24, Pages 4213-4217Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2005.04.054
Keywords
aza-Wittig reaction
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A simple and efficient method for synthesizing pyrrolines and tetrahydropyridines via an intramolecular aza-Wittig reaction has been achieved by microwave irradiation of the corresponding chloro-alkane derivatives in the presence of tertiary phosphite and sodium azide. The in situ formation of the alkyl azides makes this a facile and safe method for aza-Wittig reactions. (c) 2005 Elsevier Ltd. All rights reserved.
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