Journal
BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN
Volume 78, Issue 6, Pages 1105-1109Publisher
CHEMICAL SOC JAPAN
DOI: 10.1246/bcsj.78.1105
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The title compound was isolated for the first time by a novel procedure including dephenylbromination of cyclotetrasiloxane. The stereostructure of the tetrabromide was confirmed by condensation with diphenylsilanediol, affording anti-tricyclo[7.3.1.1(3.7)]hexasiloxane. This tetrabromide spontaneously decomposed in air to afford a white powder insoluble in organic solvents. Measurements of the TG, IR, and solid-state NMR spectra of the product revealed that a ladder polysilsesquioxane with high thermal stability and stereoregularity was obtained.
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