Journal
ORGANOMETALLICS
Volume 24, Issue 15, Pages 3624-3628Publisher
AMER CHEMICAL SOC
DOI: 10.1021/om050216f
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A new method for the synthesis of cationic Pd(IV) complexes, based on the chemical oxidation of an anionic Pd(II) metallacycle in the presence of an additional ligand, is presented. Electrochemical analysis of these compounds reveals that the stability of the +4 oxidation state is sensitive to the electron-donor capability of the added co-ligand and to the steric features of the Tp' ligand.
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