Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 70, Issue 15, Pages 6097-6100Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo050498t
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The Pd-catalyzed copper-free carbonylative Sonogashira. coupling reaction to synthesize alkynyl ketones from terminal alkynes and aryl iodides was achieved by using water as a solvent. The reaction was carried out at room temperature under balloon pressure of CO with Et3N as a base. The developed method was successfully applied to the synthesis of flavones.
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