Journal
CANADIAN JOURNAL OF CHEMISTRY
Volume 83, Issue 8, Pages 1137-1140Publisher
CANADIAN SCIENCE PUBLISHING
DOI: 10.1139/V05-134
Keywords
aromatic carboxylic esters; aromatic primary amines; secondary amides; Zn dust; microwave activation
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A mild and efficient procedure has been developed for the conversion of aromatic carboxylic esters to secondary amides using reusable Zn dust with microwave heating in the presence of N,N-dimethylformamide or conventional heating by stirring in an oil bath using THF as solvent. Zn dust can be reused several times after simple washing with dil. HCl and distilled water.
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