Journal
JOURNAL OF PHYSICAL CHEMISTRY B
Volume 109, Issue 33, Pages 16011-16016Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jp052031s
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An accurate gravimetric apparatus based on a contactless magnetic suspension microbalance was developed. This unit was used to measure the hydrogen storage capacity for a variety of carbon nanotubes (CNTs) at room temperature and hydrogen pressures up to 11.5 MPa. The results show that regardless of their synthesis methods, purities, and nanostructures all investigated CNT products possess relatively low hydrogen storage capacities (< 0.2 wt %). For comparison, the adsorption characteristics of theses samples were also measured at a pressure of 0.1 MPa and liquid nitrogen temperature (similar to 77 K) by a conventional volumetric approach. The methodological aspects related to the accuracy of the hydrogen uptake measurements are also discussed.
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