Journal
JOURNAL OF ORGANOMETALLIC CHEMISTRY
Volume 690, Issue 17, Pages 4090-4093Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/j.jorganchem.2005.05.042
Keywords
cyclometalated metal complexes; platinum; phosphorescent; 2-aryl-pyridine; crystal structure
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The one-pot reaction of K2PtCl4 and various 2-arylpyridines, HC<^>N, in a 3:1 (v/v) mixture of 2-ethoxyethanol and H2O at 80 degrees C for 16 h affords cyclometalated platinum complexes, Pt(C<^>N)(HC<^>N)(Cl), in high yield. These have been fully characterized and, in one case, the X-ray structure has been determined. (c) 2005 Elsevier B.V. All rights reserved.
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