Journal
ORGANIC LETTERS
Volume 7, Issue 18, Pages 4025-4028Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol0515255
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The total synthesis of (-)-cytoxazone 1 was achieved in six linear steps (34% overall yield) from p-anisaldehyde. The key steps in this route are the regioselective and stereoselective introduction of a N-protected amine group, using the CSI reaction of the anti-1,2-dimethyl ether 3, and the subsequent regioselective cyclization of the N-protected amino diol 13 to give the 2-oxazolidinone unit of (-)-cytoxazone 1.
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