Journal
CHEMICAL & PHARMACEUTICAL BULLETIN
Volume 53, Issue 9, Pages 1131-1135Publisher
PHARMACEUTICAL SOC JAPAN
DOI: 10.1248/cpb.53.1131
Keywords
glycocluster; omega-amino acid; D-galactose; glycodendron; unit synthesis
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The synthesis of an asymmetric glycocluster 1 has been achieved using two glycocluster units 12 and 13, prepared by coupling the cluster chain unit 4 with each omega-amino acid (beta-alanine and 6-aminocapronic acid) trichloroethyl ester, and peptidic C-terminal block glycocluster 16, prepared by,coupling the bifunctional linker 14 with sugar unit 9. This method facilitated the synthesis of the cluster optionally modulated the distance between the side-chain branched points by using various omega-amino acids. We also synthesized glycodendron 2 using the same intermediate.
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