4.5 Review

Automation of solid-phase microextraction

Journal

JOURNAL OF SEPARATION SCIENCE
Volume 28, Issue 15, Pages 2010-2022

Publisher

WILEY-V C H VERLAG GMBH
DOI: 10.1002/jssc.200500244

Keywords

automation; derivatisation; review; sample preparation; solid-phase microextraction

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This review discusses developments and future challenges in the automation of solid-phase microextraction (SPME). The emphasis of the review is placed on automated SPME-GC using fibre and in-tube configurations, and includes discussion of recent developments that may have significant implications for automation such as superelastic fibre assemblies and internally cooled fibre-SIPME. Existing methods used for automated SPME-LC are summarised together with a more detailed overview of recent developments such as using solvent desorption followed by syringe injection using a robotic system. Progress towards automation of other SPME configurations is also discussed.

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