Journal
SYNLETT
Volume -, Issue 17, Pages 2676-2678Publisher
GEORG THIEME VERLAG KG
DOI: 10.1055/s-2005-917096
Keywords
natural products; total synthesis; sulfones; condensation; hydrogenation
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A synthetic approach to sporotricale methylether, a metabolite of the fungus Sporotrichum laxum with inhibitory activity against Helicobacter pylori, is described. The synthesis relies on the condensation of 13-hydroxy-10-oxotetradecanal, prepared via reaction of a sulfone-activated moiety with valerolactone, with diethyl 3,5-dimethoxyphthalide-7-phosphonate.
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