Journal
ORGANIC LETTERS
Volume 7, Issue 22, Pages 5087-5090Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol052120n
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- NHLBI NIH HHS [HL-58114] Funding Source: Medline
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Room-temperature reduction of aromatic nitro groups to amines can be accomplished in high yield, with wide functional group tolerance and short reaction times (30 min) using a combination of palladium(11) acetate, aqueous potassium fluoride, and polymethylhydrosiloxane (PMHS). Replacing PMHS/KF with triethylsilane allows aliphatic nitro groups to be reduced to their hydroxylamines.
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