Journal
INORGANIC CHEMISTRY
Volume 44, Issue 22, Pages 7886-7894Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ic0508369
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Aromatic molecular clips bearing two symmetrically bound platinum moieties have been prepared. The molecular clip 4 readily self-assembled with linear linkers such as 4,4'-bipyridyl, 1,4-bis[2-(4-isocyano-3,5-diisopropylphenyl)ethynyl]benzene, and nicotinic acid to form molecular rectangles. The overall dimensions of the rectangle 7 were 7.3 angstrom x 15.3 angstrom. The molecular clip also self-assembled with tritopic pyridyl and isocyanide ligands to form trigonal prismatic frameworks. The characterization of the supramolecules by multinuclear NMR, electrospray mass spectrometry, and X-ray crystal structures is also reported.
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