Journal
JOURNAL OF COMBINATORIAL CHEMISTRY
Volume 7, Issue 6, Pages 968-976Publisher
AMER CHEMICAL SOC
DOI: 10.1021/cc050079+
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Diversity oriented synthesis of tricyclic compounds was achieved using a combination of the Ferrier reaction and the Pauson-Khand reaction. Ferrier reaction was effected using NbCl5, and the Pauson-Khand reaction was carried out using CO2(CO)(8), acetonitrile-dimethoxyethane. Michael additions using various alkyl, aryl, and heterocyclic thiols were also performed successfully. The Ferrier, Pauson-Khand, and Michael addition reactions were found to be highly diastereoselective.
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