Journal
EUROPEAN JOURNAL OF INORGANIC CHEMISTRY
Volume -, Issue 21, Pages 4366-4369Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/ejic.200500159
Keywords
gamma-alumina; materials science; nanostructures; solvothermal synthesis
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Boehinite [AlOOH] nanoneedles, nanorods, and nanotubes were successfully synthesized by a facile sol-hydrothermal method without using any surfactant. Calcination of the corresponding boehmite nanostructures at 700 degrees C gave the corresponding gamma-Al2O3 nanoneedles, nanorods, and nanotubes. The resulting products were characterized by XRD, TEM, HRTEM, and FT-IR spectroscopy. We found that the conditions used to produce the sol and the pH value of the hydrothermal process have important effects on the nucleation and growth of nanostructured materials. ((c) Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2005).
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