Journal
ORGANIC LETTERS
Volume 7, Issue 23, Pages 5147-5150Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol051766c
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Tert-Butyl (phenylsulfonyl)alkyl-N-hydroxycarbamates 1 have been easily prepared from aldehydes and tert-butyl N-hydroxycarbamate in a 41 methanol-water mixture using sodium benzenesulfinate and formic acid. These sulfones 1 behave as N-(Boc)-protected nitrones 4 in the reaction with organometallics to give N-(Boc)hydroxylamines. Some chemical transformations showing their interest as building blocks in organic synthesis are described.
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