Effect of processing route and second phase particles on grain refinement during equal-channel angular extrusion

The effect of coarse and fine second-phase particles on the formation of ultra-fine grained (UFG) structures have been compared during severe deformation by equal-channel angular extrusion using routes A (no rotation) and B-C (+90 degrees rotation). The presence of coarse particles has been found to increase the rate of grain refinement with route A and the homogeneity of the submicron grain structure formed, but appears less effective using route B-C. In contrast, the presence of fine dispersoids inhibits the development of new high-angle grain boundaries and the formation of an UFG structure with both routes. Retardation is far more pronounced with rotation of the sample and the dispersiod-containing alloy processed by route B-C contained mainly subgrains. The mechanisms operating in each case are discussed. (c) 2005 Elsevier B.V. All rights reserved.