Journal
JOURNAL OF MAGNETIC RESONANCE
Volume 177, Issue 2, Pages 197-202Publisher
ACADEMIC PRESS INC ELSEVIER SCIENCE
DOI: 10.1016/j.jmr.2005.07.008
Keywords
decoupling; SPINAL; 900 MHz; aligned samples; single crystals
Funding
- NCRR NIH HHS [R01RR12599, P41RR09731] Funding Source: Medline
- NIBIB NIH HHS [P41EB002031, R01EB002169] Funding Source: Medline
- NIDDK NIH HHS [DK54441] Funding Source: Medline
- NIGMS NIH HHS [P01GM56538, P01GM64676, R37GM24266, GM65833] Funding Source: Medline
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Continuous wave irradiation has limited bandwidth for heteronuclear H-1 decoupling at high fields and for C-13 decoupling in H-1/C-13/N-15 triple-resonance experiments. SPINAL-16 modulation is SPINAL16 to improve the efficiency of H-1 and C-13 heteronuclear decoupling on single crystals of peptides and oil magnetically aligned samples of membrane proteins in bicelles, which is of particular importance because aqueous samples of biomolecules are lossy at high fields, which limits the strengths of the RF fields that can be applied. (c) 2005 Elsevier Inc. All rights reserved.
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