Journal
THIN SOLID FILMS
Volume 492, Issue 1-2, Pages 88-92Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/j.tsf.2005.06.057
Keywords
zinc; nitrides; optical properties; electrochemistry
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We formed a Zn3N2 film by potentiostatic electrolysis of a zinc electrode at 1.6 V (vs. Li+/Li) in a LiCl-KCI-Li3N melt at 673 K. From the X-ray diffraction analysis, the obtained film was found to be a single phase of Zn3N2. From the X-ray photoelectron spectroscopy analysis, in the outer surface of the film, small amounts of Zn(OH)(2) and ZnO were observed, which are believed to form after electrolysis. As a result of reflectance measurement in the ultraviolet, visible and near infrared region, it was clarified that Zn3N2 has a direct band gap of 1.01 eV. (c) 2005 Elsevier B.V All rights reserved.
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