Journal
ELECTROCHEMISTRY COMMUNICATIONS
Volume 7, Issue 12, Pages 1364-1370Publisher
ELSEVIER SCIENCE INC
DOI: 10.1016/j.elecom.2005.09.020
Keywords
mesoporous metal; electrocatalyst; microchannel; lithography; platinum
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We have proposed a novel convenient pathway via solvent-evaporation-mediated direct physical casting (SEDPC) for the fabrication of mesoporous metals in a micrometer scale. We have presented the successful deposition of highly ordered mesoporous Pt into micrometer channels prepared by lithography. The direct observation by a high-resolution scanning microscope (HR-SEM) showed the formation of highly ordered 2D-hexagonal (p6mm) mesoporous metals onto such substrates. The cyclic voltammogram of the mesoporous Pt in sulfuric acid revealed a typical feature which can identify the clean Pt surface. Moreover, mesoporous Pt exhibits an effective reduction of dissolved dioxygen molecules. It is proved that mesoporous Pt deposited in a very confined area via the SEDPC method possesses electrocatalytic performance owing to Pt. (c) 2005 Elsevier B.V. All rights reserved.
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