Journal
TETRAHEDRON LETTERS
Volume 46, Issue 49, Pages 8539-8541Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2005.10.003
Keywords
2.2 '-bipyridines; cyclophanes; ring closing metathesis
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A new route to cyclophanes 6a,b incorporating 2,2'-bipyridine subunits has been elaborated using as the key steps (1) S-transalkylation of 6.6'-bis(methylsulfyl)-2,2'-bipyridines 2a,b with ethyl bromoacetate resulting in the formation of 6,6'-bis[(ethoxycarbonyl)methylsulfanyl]-2.2'-bipyridines 3a,b and (2) ring-closing metathesis of the corresponding alkenyl ethers 5a,b. (c) 2005 Elsevier Ltd. All rights reserved.
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