Journal
ORGANIC LETTERS
Volume 7, Issue 26, Pages 5837-5839Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol0523502
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[GRAPHICS] Asymmetric amination of 2,3-allenyl phosphates with nitrogen nucleophiles such as amines, hydroxylamines, and imides can be performed efficiently using a combination of zerovalent palladium complexes and SEGPHOS or MeOBlPHEP ligand, affording the corresponding optically active 1-aminated derivatives with enantiomeric excess of up to 97% ee.
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