4.4 Article

An efficient and improved procedure for preparation of triflyl azide and application in catalytic diazotransfer reaction

Journal

TETRAHEDRON LETTERS
Volume 46, Issue 52, Pages 8993-8995

Publisher

PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2005.10.103

Keywords

diazotransfer reaction; azide; amine; functional group transformation; synthesis

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An efficient and improved procedure for preparation of triflyl azide and application in catalytic diazotransfer reaction are described. The amount of highly toxic reagents NaN3 and Tf2O, is significantly reduced comparing with the previous protocol. (c) 2005 Elsevier Ltd. All rights reserved.

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