Journal
TETRAHEDRON
Volume 61, Issue 52, Pages 12386-12397Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2005.09.118
Keywords
ionic liquid phase; Hantzsch reaction; Biginelli reaction; oxidation; pyridine; polyhydroquinoline; three component synthesise; microwave
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A microwave dielectric heating assisted liquid phase synthesis of 1,4-dihydropyridines, 3,4-dihydropyrimidin-2(1H)-ones, pyridines and polyhydroquinolines using task-specific ionic liquid as a soluble support was described. The efficiency of the ionic liquid phase organic synthesis (IoLiPOS) methodology was demonstrated by using a one-pot three component condensation. The structure of the intermediates in each step was verified routinely by spectroscopic analysis and, after cleavage the target compounds were obtained in good yields and high purities. (c) 2005 Elsevier Ltd. All rights reserved.
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