Journal
ORGANIC LETTERS
Volume 8, Issue 2, Pages 187-189Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol0522889
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Since the first disclosure of difluoromethylenediphosphonate, 2, almost 40 years ago, interest in this compound has flourished in several research areas. In this paper, we present a convenient, high-yielding (99% overall) method for the preparation of milligram to multigrarn quantities of 2 (as the bis(tributylammonium salt, 2b) in a solid form that is easy to handle.
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