Journal
ORGANIC LETTERS
Volume 8, Issue 3, Pages 531-534Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol052907d
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[GRAPHICS] We have achieved a total synthesis of apratoxin A in which thiazoline formation was accomplished from the moCys containing amide 4 using PPh3(0)/Tf2O. Deprotection of the Troc and allyl ester in 17, coupling with tripeptide 3, and deprotection of the allyl ester and the Fmoc, followed by macrolactamization provided apratoxin A (1).
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