Journal
ORGANIC LETTERS
Volume 8, Issue 4, Pages 745-748Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol053010j
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A stereocontrolled approach to the preparation of the Weinreb intermediate 3 has been developed. The important features of this approach are the creation of stereogenic centers through a cyclic amino acid ester-enolate Claisen rearrangement and the use of ring-closing metathesis for the construction of the azaspirocyclic skeleton.
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