Journal
ORGANIC LETTERS
Volume 8, Issue 6, Pages 1149-1151Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol0530629
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Solid-phase Staudinger ligation of small peptides was performed on a novel core-shell-type resin. Solid-phase Staudinger ligation was mediated by synthetic solid-supported phosphinothiol, which was readily prepared by a straightforward synthetic route. This protocol afforded final peptide products in excellent yields and purities and thus could provide the opportunity to facilitate a simple manipulation for condensation of peptide fragments. In particular, the resulting resin could be recycled in a successful manner.
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