Journal
ORGANIC LETTERS
Volume 8, Issue 6, Pages 1205-1208Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol0600741
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A convergent synthesis of the right-hand half of ciguatoxin (the HIJKLM ring system) has been achieved with complete stereocontrol in the introduction of the stereocenters on the eight-membered I ring. Key steps are Sonogashira coupling, dicobalt complexation, intramolecular conjugate addition, and hydrogenation of an endo-olefin to provide the 39-alpha-methyl group.
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