Journal
ORGANIC LETTERS
Volume 8, Issue 7, Pages 1295-1297Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol0530326
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Catalytic asymmetric allylation of 3,4-dihydro-6,7-dimethoxyisoquinoline was carried out using allyltrimethoxysilane in the presence of Cu(I) and tol-BINAP. The allyl adduct thus obtained was transformed to a chiral synthetic intermediate for (-)-emetine in good yield. The procedure was applied to the total synthesis of ent-emetine.
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