Journal
JOURNAL OF ALLOYS AND COMPOUNDS
Volume 414, Issue 1-2, Pages 224-229Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/j.jallcom.2005.07.011
Keywords
ferroelectrics; sol-gel synthesis; X-ray diffraction; thermal analysis
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Lead zirconate titanate (PZT) (53/47) powders were prepared by a cheating acetate sol-gel process. The drying temperature effect on crystallization behavior was conducted to determine the best conditions for preparing high content of perovskite PZT powders in the morphotropic region. DSC/TG analysis, Fr-IR spectrum and X-ray diffraction were carried out to identify the reaction sequences and calculated the activation energy of every transition temperature during the drying procedures. In the present work, well-crystallized, single-phase perovskite PZT powders were obtained after drying PZT stock solution at 300 degrees C for 1 h, then heat treatment at 600 degrees C for 30 min. The dependence of this crystallization temperature on the drying conditions was discussed. (c) 2005 Elsevier B.V. All rights reserved.
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