Journal
ORGANIC LETTERS
Volume 8, Issue 9, Pages 1815-1818Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol0603155
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A series of glycosyl phosphates were prepared in high yield by treatment of the corresponding 1,2-orthoesters with dibutyl phosphate. Glycosyl phosphates are efficient glycosylating agents even when used in crude form or when generated in situ. The immunodominant epitope trirhamnoside of group B Streptococcus was prepared to demonstrate the synthetic utility of the method.
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