Journal
ORGANIC LETTERS
Volume 8, Issue 9, Pages 1771-1773Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol0600234
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A general, high yielding rapid iron-catalyzed cross-coupling reaction between Grignard reagents and imidoyl chlorides is described. These reactions are typically completed within 5 min, resulting in high yields of 71-96% using 5% iron catalyst in a THF-NMP solvent mixture. Functionalized imidoyl chlorides (e.g., R = CO2Me) gave excellent yields (89%).
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