Journal
JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS
Volume 67, Issue 5-6, Pages 1173-1177Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.jpcs.2006.01.043
Keywords
inorganic compounds; X-ray diffraction; electrochemical properties; electron paramagnetic resonance (EPR); nuclear magnetic resonance (NMR)
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In order to better understand the low faradic yield of low temperature fluorinated graphite used as electrode in primary lithium batteries, a study of the discharge mechanism has been performed. The evolution of some physico-chemical parameters such as C-F bond nature and structure of the fluorocarbon matrix has been determined by X-ray diffraction, solid state F-19 NMR and EPR as a function of the depth of discharge. The influence of residual catalytic species on electrochemical properties will be also discussed. (c) 2006 Elsevier Ltd. All rights reserved.
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