Journal
TETRAHEDRON LETTERS
Volume 47, Issue 18, Pages 3055-3058Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tetlet.2006.03.007
Keywords
1,4-disubstittited 1 2,3-triazoles; 1,3-dipolar cycloaddition; PEG; water; CuI
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An efficient method is described for the regioselective synthesis of 1,4-disubstituted 1,2,3-triazoles in high yields from a variety of Baylis-Hillman acetates and terminal alkynes with sodium azide using CUI as a catalyst, in either water or polyethylene glycol (PEG). This procedure is operationally simple and environmentally benign. Polyethylene glycol (PEG) serves as an efficient reusable solvent with higher efficiency. (c) 2006 Elsevier Ltd. All rights reserved.
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