Journal
ORGANIC LETTERS
Volume 8, Issue 13, Pages 2787-2790Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ol060871z
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An unexpected one-pot synthetic approach toward spiro[fluorene-9,9'-xanthene] (SFX) under excessive MeSO3H conditions has been developed. The key step involves a thermodynamically controlled cyclization reaction. Blue-light-emitting materials based on SFX building blocks that exhibit high thermal stability have also been synthesized.
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