Journal
JOURNAL OF MATERIALS RESEARCH
Volume 21, Issue 7, Pages 1658-1663Publisher
CAMBRIDGE UNIV PRESS
DOI: 10.1557/JMR.2006.0209
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Carbon nitrogen nanotubes and nanofibers with controlled nitrogen concentration have been prepared by reaction of cyanuric chloride and hexachlorobenzene (HCB) with sodium metal at 250 degrees C in cyclohexane. Electron microscopy and spectroscopic analysis were used to characterize the products. The total yields of the tubes and fibers decrease as the ratio of cyanuric chloride to HCB increases, and nitrogen content in the products could be controlled by the ratio. The nanostructures depended strongly on the nitrogen content. Lower nitrogen content was favorable for producing linear products.
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